Fluorinated Surfaces, Coatings, and Films by David G. Castner, David W. Grainger

By David G. Castner, David W. Grainger

This publication is targeted on contemporary learn into constructing lower-cost fluorinated polymers to be used within the advertisement polymer industry.

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19 3 l 6 F8H2PC/F8H2 Vesicles. 5 mL) (total concentration of membrane components = 40 mM), and the solvent was removed by rotoevaporation. The resulting film was hydrated by the appropriate solution (water or Hepes buffer, containing C F or not) for 1 h at 40°C, then submitted to brief sonication (2 min) at the same temperature. A homogenous population of vesicles was formed as seen by L L S spectroscopy. Carboxyfluorescein Entrapment and Release Experiments. 5). They were annealed by incubation for 12h at 50°C in order to remove the defects present in the membrane as a result of sonication.

15 M NaCl as the eluent (27). ; ACS Symposium Series; American Chemical Society: Washington, DC, 2001. ch004 Release of the entrapped C F was monitored using fluorescence spectroscopy. This method exploits the self-quenching of the fluorescence of C F when confined at high concentration in the internal space of vesicles (22). Release of CF through the bilayer membrane results in its dilution and consequent build-up of fluorescence. After removing the non-entrapped dye, 5 uL of the dispersion of vesicles were placed in a cuvette containing 2 mL of saline buffer.

The (√3 x √3) R 30° lattice structure was proved by electron diffraction (Chidsey, C. E . ; Loiacono, D . N. ; Chidsey, C. E . ; Putvinski, T. ; Scoles, G. J. Chem. Phys. 1991, 94, 8493). ; Salmeron, M. Langmuir 1994, 10, 367. ; Whitesides, G. M. Langmuir 1988, 4, 546. Dialkyl thioethers were shown to form a (√3 x √3) R 30° lattice which is indistinguishable from n-alkane thiols. However, Strong and Whitesides (reference 7) attributed the observed structure to thiol impurities. More recently it was shown that highly purified dialkyl thioethers (e.

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